PART 1 INTRODUCTION TO THE ORGANIC LABORATORY
ESSAY: The Role of the Laboratory
1. Safety in the Laboratory
2. Protecting the Environment
3. Laboratory Notebooks and Prelaboratory Information
PART 2: CARRYING OUT CHEMICAL REACTIONS
ESSAY: Learning to Do Organic Chemistry
4. Laboratory Glassware
5. Measurements and Transferrign Reagents
6. Heating and Cooling Methods
7. Assembling a Reaction Apparatus
8. Computational Chemistry
9. Planning a Chemical Reaction
PART 3 SEPARATION AND PURIFICATION TECHNIQUES
ESSAY: Intermolecular Forces in Organic Chemistry
10. Filtration
11. Extraction
12. Drying Organic Liquids and Recovering Reaction Products
13. Boiling Points and Distillation
14. Melting Points and Melting Ranges
15. Recrystallization
16. Specialized Techniques
PART 4 CHROMOTOGRAPHIC SEPARATION AND ANALYSES
ESSAY: Modern Chromatographic Separations
17. Thin-Layer Chromatography
18. Liquid Chromotography
19. Gas-Liquid Chromotography
PART 5 SPECTROSCOPIC METHODS
ESSAY: The Spectroscopic Revolution
20. Infrared Spectroscopy
21. 1H Nuclear Magnetic Resonance Spectroscopy
22. 13C and Two-Dimensional NMR Spectroscopy
23. Mass Spectrometry
24. Ultraviolet and Visible Spectroscopy
25. Integrated Spectroscopy Problems